Introduction
Humidity Measurement in Tantalum Capacitor Pyrolysis Furnaces
In tantalum capacitor manufacturing, there is a steam pyrolysis process where tantalum pellets are decomposed by steam. Humidity control in this process is important to maintain product quality and improve yield.
Stable humidity measurement at high temperatures of 200 to 400 °C is required. The ZR802G Zirconia High Temperature Humidity Analyzer is easy to maintain because of direct insertion in process without sampling system and utilizes a long-life sensor with fast response. It is widely used in humidity instrumentation applications and has been well received in the marketplace.
Expected Benefits
- Maintains the quality of the tantalum capacitor manufacturing process
- Ensures stable, continuous humidity measurement
- Reduces operating costs
Process Overview
A tantalum pellet with an electrode plate applied is immersed in a manganese nitrate solution. This dipping process allows the manganese nitrate to penetrate the porous part of the pellet. After dipping, the pellet is forwarded to the pyrolysis process where the manganese nitrate is decomposed under high temperature and humidity conditions to form a manganese dioxide coating by the reaction Mn(NO3)2 -> MnO2 + 2NO2. These steps are repeated until the coating is sufficient. To improve the coating uniformity and yield, the humidity is controlled.
Steam Pyrolysis Process in Tantalum Capacitor Manufacturing
Solution Details
Field Data
Process conditions
Measurement point | Inside the steam pyrolysis furnace |
---|---|
Temperature | 200 to 400°C |
Pressure | 10 to 20 Pa |
Humidity | 25 to 80 vol%H2O |
Dust | None |
Measurement system
Detector | ZR22G-☐☐☐-S-☐-C-R-☐-E-A/SV |
---|---|
Converter | ZR802G-☐-☐-N-N /☐ |
Flow Setting Unit | ZA8F-J*C |
Utilities
Rated voltage | 100 to 240 V AC |
---|---|
Rated frequency | 50/60 Hz |
Power consumption | 330 VA (Max. 800 VA) |
Notes on Installation: As the sensor inside a pyrolysis furnace is hot, it can be easily damaged if cooler water drips onto it. The sensor should be installed with the probe head pointing downward.
Related Products & Solutions
-
Zirconia Oxygen/Humidity Analyzer ZR22G, ZR802G
This Oxygen concentration and humidity at high temperatures consists of a ZR22G detector equipped with a long-life and highly reliable zirconia sensor, and a converter ZR802G equipped with digital communication and data log functions.
ZR22G and ZR802G can be measured directly and continuously without a sampling device. It is easy to maintain and reduce operating costs by self-diagnosis of sensor deterioration (without using calibration gas )and replacing the heater assembly on site.
Have Questions?
Contact a Yokogawa Expert to learn how we can help you solve your challenges.